(cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate)

Base Information

Chemical Name:(cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate)
CAS No.:554408-97-8
Molecular Formula:C₁₃H₉FeN₅O₂
Molecular Weight:323.094
Hs Code.:

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Chemical Property of (cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate)

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Technology Process of (cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate)

There total 1 articles about (cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 152572-89-9
[Fe(CO)2(tetrahydrofuran)(Cp)]SO₃CF₃

: 14389-12-9
4-(1H-tetrazol-5-yl)-pyridine

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 554408-97-8
(cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate)

Guidance literature:: With triethylamine; In methanol; Ar; dropwise addn. of iron complex in methanol to methanolic soln. of the ligand contg. triethylamine, stirring of the suspn. at room temp. for 6 h; filtration (Celite pad), evapn. to dryness, chromy. (alumina, dichloromethane-acetonitrile 5:1); elem. anal.;
DOI:10.1016/S0022-328X(03)00002-0

Reference yield: 70.0%

: 554408-97-8
(cyclopentadienyl)Fe(carbonyl)2(5-(4-pyridyl)-tetrazolate)

: 333-27-7
methyl trifluoromethanesulfonate

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 554408-99-0
[(cyclopentadienyl)Fe(carbonyl)2(4-(methyl)N₄C-C₅H₄N)] triflate

Guidance literature:: In dichloromethane; Ar; addn. of methyl triflate to dichloromethane soln. of the iron complex, stirring at -30°C for 30 min, warming up to room temp., stirring for 3 h; evapn. of the solvent, chromy. (alumina, CH2Cl2 followed by CH2Cl2-CH3CN, 2:1 vol.); elem. anal.;
DOI:10.1016/S0022-328X(03)00002-0