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Azido-PEG1-CH2CO2tBu

Base Information Edit
  • Chemical Name:Azido-PEG1-CH2CO2tBu
  • CAS No.:1820717-35-8
  • Molecular Formula:C8H15N3O3
  • Molecular Weight:201.225
  • Hs Code.:
  • Mol file:1820717-35-8.mol
Azido-PEG1-CH2CO2tBu

Synonyms:

Suppliers and Price of Azido-PEG1-CH2CO2tBu
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • Azido-PEG1-CH2CO2-t-butylEster
  • 5mg
  • $ 45.00
  • BroadPharm
  • Azido-PEG1-CH2CO2-t-Bu 98%
  • 250 MG
  • $ 250.00
  • Acrotein
  • tert-Butyl2-(2-azidoethoxy)acetate 97%
  • 1g
  • $ 495.00
Total 11 raw suppliers
Chemical Property of Azido-PEG1-CH2CO2tBu Edit
Chemical Property:
  • Solubility.:Soluble in DCM, DMF 
Purity/Quality:

99.3% *data from raw suppliers

Azido-PEG1-CH2CO2-t-butylEster *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
  • Description Azido-PEG1-CH2CO2-t-Bu is a azide (N3) containing PEG linker.The azide group can react with alkyne, BCN, DBCO via Click Chemistry to yield a stable triazole linkage. The t-butyl protected carboxyl group can be deprotected under acidic conditions.
Technology Process of Azido-PEG1-CH2CO2tBu

There total 5 articles about Azido-PEG1-CH2CO2tBu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium azide; In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1021/acsmedchemlett.9b00025
Guidance literature:
With sodium hydride; In tetrahydrofuran; at 20 ℃; for 3.66667h; Cooling with ice;
Guidance literature:
Multi-step reaction with 4 steps
1.1: potassium tert-butylate / tert-butyl alcohol / 0.5 h / 20 °C
1.2: 16 h / 10 - 20 °C
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h
3.1: dmap; triethylamine / dichloromethane / 20 °C
4.1: sodium azide / N,N-dimethyl-formamide / 100 °C
With dmap; sodium azide; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/acsmedchemlett.9b00025
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