[Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2

Base Information

Chemical Name:[Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2
CAS No.:894354-51-9
Molecular Formula:C₅₄H₇₀Cu₂I₂N₆O₄
Molecular Weight:1248.09
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2

Chemical Property:

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Technology Process of [Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2

There total 1 articles about [Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2*2CH3OH

: 80937-33-3
oxygen

: 894354-51-9
[Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2

Guidance literature:: In dichloromethane; dry O2 bubbled into stirring soln. of Cu complex in anhyd. CH2Cl2 for 10-20 min at 193 K; not isolated; generated in situ;
DOI:10.1039/b513898a

Reference yield: 35.0%

: 75-09-2
dichloromethane

: 894354-51-9
[Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2

: 603-35-0
triphenylphosphine

: [Cu(PPh₃)3I]*CH₂Cl₂

Guidance literature:: In dichloromethane; byproducts: OP(C6H5)3; stream of Ar was purged into soln. of Cu complex at 193 K for 15 min; excess of PPh3 in CH2Cl2 added; mixt. stirred at 193 K for 10 min; soln. warmed to room temp.; soln. allowed to stand at room temp. for a few ds; crystals isolated; washed (Et2O); dried (vac.); elem. anal.;
DOI:10.1039/b513898a

Reference yield:

: tetrafluoroboric acid

: 894354-51-9
[Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2O2

: 894354-50-8
[Cu([N-(3,5-di-tert-butyl-2-hydroxybenzyl)-N,N-di-(2-pyridylmethyl)]amine)(μ-I)]2

: 7722-84-1
dihydrogen peroxide

Guidance literature:: In diethyl ether; dichloromethane; soln. of Cu complex in CH2Cl2 cooled to 193 K; treated with excess HBF4/Et2O;
DOI:10.1039/b513898a