(S)-N¹-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate)

Base Information

• Chemical Name: (S)-N¹-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate)
• CAS No.: 909786-44-3
• Molecular Formula: C₂HF₃O₂*C₃₀H₅₂N₁₀O₇
• Molecular Weight: 778.83

Synonyms:

Chemical Property of (S)-N¹-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate)

Chemical Property:

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Technology Process of (S)-N¹-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate)

There total 1 articles about (S)-N¹-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-(tert-butoxycarbonylamino)-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid (186698-61-3) + 2-(trimethylsilyl)ethyl 5-aminopentylcarbamate (1260636-97-2) + N-[(o-nitrophenyl)sulfonyl]-β-alanine (90558-39-7) + 2-(2,4-bis(benzyloxy)phenyl)acetic acid (66056-40-4) + L-Asn(Trt) (132388-59-1) + trifluoroacetic acid (76-05-1) + 4-{N-[2-(Trimethylsilyl)ethoxycarbonyl]amino}butanol (351016-76-7) → (S)-N1-((S)-1,5-diamino-1-imino-6,15-dioxo-2,7,12,16-tetraazahenicosan-21-yl)-2-(2-(2,4-dihydroxyphenyl)acetamido)-succinamide tris(2,2,2-trifluoroacetate) (909786-44-3)

Guidance literature:

2-(trimethylsilyl)ethyl 5-aminopentylcarbamate; With 2-(3,5-dimethoxy-4-formylphenoxy)ethyl polystyrene; In acetic acid; N,N-dimethyl-formamide; for 0.0333333h; 2-(3,5-dimethoxy-4-formylphenoxy)ethyl polystyrene

With sodium tris(acetoxy)borohydride; In acetic acid; N,N-dimethyl-formamide; at 20 ℃; 2-(3,5-dimethoxy-4-formylphenoxy)ethyl polystyrene

(S)-2-(tert-butoxycarbonylamino)-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid; N-[(o-nitrophenyl)sulfonyl]-β-alanine; 2-(2,4-bis(benzyloxy)phenyl)acetic acid; L-Asn(Trt); trifluoroacetic acid; 4-{N-[2-(Trimethylsilyl)ethoxycarbonyl]amino}butanol; Further stages;

DOI:10.1021/jm301255m

upstream raw materials:

(S)-2-(tert-butoxycarbonylamino)-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid

2-(trimethylsilyl)ethyl 5-aminopentylcarbamate

N-[(o-nitrophenyl)sulfonyl]-β-alanine

2-(2,4-bis(benzyloxy)phenyl)acetic acid

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