9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine

Base Information

• Chemical Name: 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine
• CAS No.: 26422-89-9
• Molecular Formula: C₁₇H₁₃N₃
• Molecular Weight: 259.31
• Mol file: 26422-89-9.mol

Synonyms:

Chemical Property of 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine

There total 4 articles about 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine (26422-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / N,N-dimethyl-formamide / 24 h / 75 °C

2: tetrahydrofuran / 3 h / UV-irradiation

With sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1039/c8dt03912g

Reference yield:

di(pyridin-2-yl)amine (1202-34-2) → 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine (26422-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / N,N-dimethyl-formamide / 24 h / 75 °C

2: tetrahydrofuran / 3 h / UV-irradiation

With sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1039/c8dt03912g

Reference yield:

N-benzyl-N-(pyridin-2-yl)pyridine-2-amine (26422-90-2) → 9-benzyl-9H-pyrrolo[2,3-b;5,4-b']dipyridine (26422-89-9)

Guidance literature:

In tetrahydrofuran; for 3h; Time; Solvent; UV-irradiation;

DOI:10.1039/c8dt03912g

upstream raw materials:

di(pyridin-2-yl)amine

N-benzyl-N-(pyridin-2-yl)pyridine-2-amine

benzyl bromide