Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2

Base Information

Chemical Name:Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2
CAS No.:380456-20-2
Molecular Formula:C₃₄H₃₀B₂ClF₂FeN₇O₆
Molecular Weight:783.574
Hs Code.:

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Chemical Property of Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2

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Technology Process of Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2

There total 1 articles about Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 380456-14-4
FeBd2(Cl2Gm)(BF)2

: 109-89-7
diethylamine

: 380456-20-2
Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2

Guidance literature:: In N,N-dimethyl-formamide; Fe-contg. compd. (1 mmol) and an excess of diethylamine were dissolved/suspended in dry DMF and left overnight; then the react. mixt. was stirred for 7 h at 50°C; solid was pptd. with H2O; it was filtered off and repptd. from DMF soln.with satd. aq. NaClO4 soln.; it was washed with H2O and MeOH, and dried in vac.; the soln. in CHCl3 was filtered and evapd. to dryness; washing with CHCl3 and hexane; elem. anal.;
DOI:10.1039/b107021p

Reference yield: 22.0%

: 380456-20-2
Fe(α-benzyldioximato)2((Et2N)ClGm)(BF)2

: 462-94-2
1,5-diaminopentane

: Fe(α-benzyldioximato)2((Et2N)(NH2(CH2)5NH)Gm)(BF)2

Guidance literature:: In N,N-dimethyl-formamide; Fe-contg. compd. (0.3 mmol) and an excess of cadaverine were dissolved/suspended in dry DMF and left overnight; solid was pptd. with H2O; it was filtered off and repptd. from DMF soln.with satd. aq. NaClO4 soln.; it was washed with MeOH-H2O mixt. and drie d in vac.; the soln. in CHCl3 was passed through Silasorb SPH-300; elution with MeCN-CHCl3 mixt.; elem. anal.;
DOI:10.1039/b107021p