Technology Process of bis-(triphenylphosphine)iminium-bis-t-butoxophthalocyaninatoferrate(III)
There total 3 articles about bis-(triphenylphosphine)iminium-bis-t-butoxophthalocyaninatoferrate(III) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium; tert-butyl alcohol;
In
dichloromethane;
byproducts: KClO4; addn. of of a K-alcoholate-soln. (prepd. by dissolving of K in the alcohol) to a suspension of the P-compd. and the Fe-compd. (prepd. by oxidn.of Fe-phthalocyanine with Br2 in CH2Cl2), stirring for 15 min. at room temp.; pptd. KClO4 is filtered off, addn. of anhyd. ether to the soln. until beginning of crystn., standing a longer time at -25°C;
- Guidance literature:
-
With
potassium; tert-butyl alcohol;
In
dichloromethane;
byproducts: KClO4; addn. of of a K-alcoholate-soln. (prepd. by dissolving of K in the alcohol) to a suspension of the P-compd. and the Fe-compd. (prepd. by oxidn.of Fe-phthalocyanine with Cl2 in CH2Cl2), stirring for 15 min. at room temp.; pptd. KClO4 is filtered off, addn. of anhyd. ether to the soln. until beginning of crystn., standing a longer time at -25°C;
- Guidance literature:
-
With
potassium; tert-butyl alcohol;
In
dichloromethane;
byproducts: KClO4; addn. of of a K-alcoholate-soln. (prepd. by dissolving of K in the alcohol) to a suspension of the P-compd. and the Fe-compd., stirring for 15 min. at room temp.; pptd. KClO4 is filtered off, addn. of anhyd. ether to the soln. until beginning of crystn., standing a longer time at -25°C;
