(1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one

Base Information

• Chemical Name: (1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one
• CAS No.: 100924-13-8
• Molecular Formula: C₃₂H₅₉NO₇SSi₃
• Molecular Weight: 686.145

Synonyms:

Chemical Property of (1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one

There total 1 articles about (1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tosyl isocyanate (4083-64-1) + tri-O-(tert-butyldimethylsilyl)-D-glucal (79999-47-6) → (1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one (100924-13-8)

Guidance literature:

In diethyl ether; for 20h; Ambient temperature;

DOI:10.1016/S0040-4020(01)96639-6

Reference yield: 70.0%

methanol (67-56-1) + (1S,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(tert-butyl-dimethyl-silanyloxymethyl)-8-(toluene-4-sulfonyl)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one (100924-13-8) → N-[(2R,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxy-tetrahydro-pyran-3-carbonyl]-4-methyl-benzenesulfonamide (100933-65-1)

Guidance literature:

for 1h; Ambient temperature;

DOI:10.1016/S0040-4020(01)96639-6

upstream raw materials:

Tosyl isocyanate

tri-O-(tert-butyldimethylsilyl)-D-glucal

Downstream raw materials:

N-[(2R,3R,4R,5R,6R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-6-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxy-tetrahydro-pyran-3-carbonyl]-4-methyl-benzenesulfonamide

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