methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate

Base Information

• Chemical Name: methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate
• CAS No.: 134039-46-6
• Molecular Formula: C₂₃H₂₃N₃O₁₃S₂
• Molecular Weight: 613.58

Synonyms:

Chemical Property of methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate

There total 3 articles about methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

silver(I) acetate (563-63-3) + methyl 5-cyclohexa-1,3-diene-1-carboxylate (134039-35-3) → methyl 4α-acetoxy-3α-hydroxy-5β-cyclohex-1-ene-1-carboxylate (134039-45-5) + methyl 3α-acetoxy-4α-hydroxy-5β-cyclohex-1-ene-1-carboxylate (134039-46-6,145264-69-3) + methyl 3α,4α-diacetoxy-5β-cyclohex-1-ene-1-carboxylate (145214-91-1,145264-68-2) + methyl 3β,4α-diacetoxy-5β-cyclohex-1-ene-1-carboxylate (145214-91-1,145264-68-2)

Guidance literature:

With iodine; In acetic acid; for 2h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1016/S0040-4020(01)89449-7

Reference yield:

silver(I) acetate (563-63-3) + methyl 5-cyclohexa-1,3-diene-1-carboxylate (134039-35-3) → methyl 3α-acetoxy-4α-hydroxy-5β-cyclohex-1-ene-1-carboxylate (134039-46-6,145264-69-3) + methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate (134039-46-6,145264-69-3) + methyl 3α,4α-diacetoxy-5β-cyclohex-1-ene-1-carboxylate (145214-91-1,145264-68-2) + methyl 3β,4α-diacetoxy-5β-cyclohex-1-ene-1-carboxylate (145214-91-1,145264-68-2)

Guidance literature:

With iodine; In acetic acid; for 2h; Yield given. Further byproducts given. Yields of byproduct given; Heating;

DOI:10.1016/S0040-4020(01)89449-7

Reference yield:

silver(I) acetate (563-63-3) + methyl 5-cyclohexa-1,3-diene-1-carboxylate (134039-35-3) → methyl 3α-acetoxy-4α-hydroxy-5β-cyclohex-1-ene-1-carboxylate (134039-46-6,145264-69-3) + methyl 3β-acetoxy-4β-hydroxy-5β-cyclohex-1-ene-1-carboxylate (134039-46-6,145264-69-3) + methyl 3α,4α-diacetoxy-5β-cyclohex-1-ene-1-carboxylate (145214-91-1,145264-68-2) + methyl 3β,4α-diacetoxy-5β-cyclohex-1-ene-1-carboxylate (145214-91-1,145264-68-2)

Guidance literature:

With iodine; In acetic acid; for 2h; Yield given. Further byproducts given. Yields of byproduct given; Heating;

DOI:10.1016/S0040-4020(01)89449-7

upstream raw materials:

silver(I) acetate

methyl 5-cyclohexa-1,3-diene-1-carboxylate

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