GeCl₃COC₆H₅

Base Information

Chemical Name:GeCl₃COC₆H₅
CAS No.:83447-99-8
Molecular Formula:C₇H₅Cl₃GeO
Molecular Weight:284.065
Hs Code.:

GeCl<sub>3</sub>COC<sub>6</sub>H<sub>5</sub>

Synonyms:

Suppliers and Price of GeCl₃COC₆H₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of GeCl₃COC₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of GeCl₃COC₆H₅

There total 1 articles about GeCl₃COC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 623-73-4
diazoacetic acid ethyl ester

: 10038-98-9
germaniumtetrachloride

: 100-52-7
benzaldehyde

: 83447-99-8
GeCl₃COC₆H₅

Guidance literature:: In pentane; byproducts: ClCH2COOCH2CH3, C6H5COCl, C6H5COCOC6H5; diazoester adding slowly to a mixt. of C6H5CHO and GeCl4 in pentane in a molar ratio 1:1:1, reacting for 14 h at 20°C and distg. in vacuo; not isolated in a pure form; identified by IR spectrum;
DOI:10.1016/S0022-328X(00)87640-8

Reference yield:

: 83447-99-8
GeCl₃COC₆H₅

: 100-58-3
phenylmagnesium bromide

: 4639-78-5
α-triphenylgermanyl-benzhydrol

Guidance literature:: In further solvent(s); PhMgBr in ether adding in excess to a mixt. of trichlorogermylketone with PhCOCH2CO2C2H5; identified by elem. anal.;
DOI:10.1016/S0022-328X(00)87640-8