(TMPP)MnOAc

Base Information

Chemical Name:(TMPP)MnOAc
CAS No.:101565-35-9
Molecular Formula:C₅₀H₃₉MnN₄O₆
Molecular Weight:846.821
Hs Code.:

Synonyms:

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Chemical Property of (TMPP)MnOAc

Chemical Property:

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Technology Process of (TMPP)MnOAc

There total 2 articles about (TMPP)MnOAc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5,10,15,20-meso-tetra(p-methoxyphenyl) porphyrin

: 638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3
manganese(II) acetate

: 101565-35-9
(TMPP)MnOAc

Guidance literature:: In N,N-dimethyl-formamide; by reflux free base with excess Mn(CH3COO)2 in DMF (according to James,B. R. In The Porphyrins; Dolphin, D. E., Ed.; Academic: New York, 1978;vol. 5, Chapter 6);; the product was dissolved in benzene and treated with aq. NaCl; purifn.by recrystn. from benzene-heptane; the final product was found to be pure by TLC (silica gel, CH2Cl2) and visible spectroscopy;;

Reference yield:

: 638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3
manganese(IV) acetate

: 22112-78-3
5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin

: 101565-35-9
T(4-OMeP)PMnOAc

Guidance literature:: DOI:10.1142/S1088424610002136

Reference yield:

: 532-32-1
sodium benzoate

: 101565-35-9
(TMPP)MnOAc

: 109282-73-7
manganese(III) tetrakis(p-methoxyphenyl)porphyrin benzoate

Guidance literature:: In dichloromethane; water; a soln. of Mn-compd. in CH2Cl2 was treated with a dil. aq. soln. of NaC6H5COO; the procedure was repeated, followed by a final wash with distd.water; the org.layer was collected, dried over anhyd. Na2SO4, then reduced to 5 ml under reduced pressure;; crystn. by slow addn. of heptane; purity was confirmed by visible spectroscopy and cyclic voltammetric behavior;;