(2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II)

Base Information

Chemical Name:(2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II)
CAS No.:102777-48-0
Molecular Formula:C₅₃H₆₁FeN₇O₄S₂
Molecular Weight:980.091
Hs Code.:

Synonyms:

Suppliers and Price of (2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II)

There total 1 articles about (2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: octaethylverdohemochrome

: 7664-41-7
ammonia

: 79047-38-4
isocyanomethyl p-toluenesulfonate

: 102777-48-0
(2,3,7,8,12,13,17,18-octaethyl-5-aza-porphyrinato)bis(tosyl methylisocyanide)iron(II)

Guidance literature:: In methanol; dichloromethane; ammonia; addn. of a concd. NH3 solution (10 ml) under Ar to a solution of the bis-pyridine complex (0.21 mmol) in 2 ml CH2Cl2 and 10 ml MeOH, storing overnight, extraction (CH2Cl2), evaporation, dissolving together with CH3C6H4SO2CH2NC (2.6 mmol) in 5 ml CH2Cl2;; chromatography (CH2Cl2/MeOH), recrystallization from CH2Cl2/light petroleum; elem. anal.;;