Zn₄(SC₆H₂(CH(CH₃)2)3)4(OCH₂(C₃N₂H₂)CH₃)3(OCH₃)

Base Information

• Chemical Name: Zn₄(SC₆H₂(CH(CH₃)2)3)4(OCH₂(C₃N₂H₂)CH₃)3(OCH₃)
• CAS No.: 366792-31-6
• Molecular Formula: C₇₆H₁₁₆N₆O₄S₄Zn₄
• Molecular Weight: 1567.62
• Mol file: 366792-31-6.mol

Synonyms:

Chemical Property of Zn₄(SC₆H₂(CH(CH₃)2)3)4(OCH₂(C₃N₂H₂)CH₃)3(OCH₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Zn₄(SC₆H₂(CH(CH₃)2)3)4(OCH₂(C₃N₂H₂)CH₃)3(OCH₃)

There total 1 articles about Zn₄(SC₆H₂(CH(CH₃)2)3)4(OCH₂(C₃N₂H₂)CH₃)3(OCH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

1-methyl-2-hydroxymethylimidazole (17334-08-6) + 2,4,6-Triisopropylthiophenol (22693-41-0) + diethylzinc (557-20-0) → Zn4(SC6H2(CH(CH3)2)3)4(OCH2(C3N2H2)CH3)3(OCH3) (366792-31-6)

Guidance literature:

In tetrahydrofuran; methanol; hexane; all manipulations with exclusion of air and moisture; soln. of Et2Zn in hexane slowly, dropwise added to soln. of org. compds. in 1:1 THF/MeOH, then stirred at room temp. for 1 h; volatiles removed in vac., residue dissolved in abs. CH2Cl2, layered with hexane, cocrystallyzed solvent removed in vac.; elem. anal.;

DOI:10.1002/1521-3749(200108)627:8<1771::aid-zaac1771>3.0.co;2-1

upstream raw materials:

1-methyl-2-hydroxymethylimidazole

2,4,6-Triisopropylthiophenol

diethylzinc