4-ferrocenylbenzylacetate

Base Information

• Chemical Name: 4-ferrocenylbenzylacetate
• CAS No.: 1157855-00-9
• Molecular Formula: C₁₉H₁₈FeO₂
• Molecular Weight: 334.198
• Mol file: 1157855-00-9.mol

Synonyms:

Chemical Property of 4-ferrocenylbenzylacetate

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 4-ferrocenylbenzylacetate

There total 1 articles about 4-ferrocenylbenzylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

potassium tetrachloroplatinate(II) (10025-99-7) + 4-ferrocenylbenzyl-1H-imidazole-1-carboxylate (1157854-68-6) + acetone (67-64-1) → 4-ferrocenylbenzylacetate (1157855-00-9) + dichlorobis(4-ferrocenylbenzyl-1H-imidazole-1-carboxylate)platinum

Guidance literature:

In dichloromethane; water; acetone; soln. of K2PtCl4 in H2O-acetone stirred for 15 min; soln. of Fe complex in CH2Cl2 added dropwise; shaken; stirred overnight; org. layer sepd.; dried (anhyd. Na2SO4); filtered; concd.; susbjected tocolumn chromy. (silica gel, ethyl acetate); orange band collected; crys td. by slow evapn.; elem. anal.;

DOI:10.1016/j.jorganchem.2008.12.041

upstream raw materials:

potassium tetrachloroplatinate(II)

4-ferrocenylbenzyl-1H-imidazole-1-carboxylate

acetone