3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester

Base Information

• Chemical Name: 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester
• CAS No.: 30286-95-4
• Molecular Formula: C₂₁H₂₁NO₅
• Molecular Weight: 367.401

Synonyms:

Chemical Property of 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester

Chemical Property:

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Useful:

Technology Process of 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester

There total 2 articles about 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid anhydride (16108-74-0,30286-94-3) → 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester (30286-95-4)

Guidance literature:

With sulfuric acid; Heating;

DOI:10.1016/S0040-4020(01)93164-3

Reference yield:

9,10-dimethoxycarbonyltricyclo<4.2.2.02,5>deca-3,7-diene (35211-83-7) + benzohydroximoyl chloride (698-16-8) → 3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid dimethyl ester (30286-95-4)

Guidance literature:

Multistep reaction; (i) aq. NaOH, CHCl₃, (ii) /BRN= 3215443/;

DOI:10.1016/S0040-4020(01)93164-3

upstream raw materials:

methanol

3-phenyl-(3ac,3bt,7at,7bc)-3a,3b,4,5,6,7,7a,7b-octahydro-4r,7c-etheno-benzo[3,4]cyclobuta[1,2-d]isoxazole-5c,6c-dicarboxylic acid anhydride

9,10-dimethoxycarbonyltricyclo<4.2.2.0^2,5>deca-3,7-diene

benzohydroximoyl chloride

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