2,2':6',2''-Terpyridine, 4'-(3,4-dimethoxyphenyl)-

Base Information

• Chemical Name: 2,2':6',2''-Terpyridine, 4'-(3,4-dimethoxyphenyl)-
• CAS No.: 142719-61-7
• Molecular Formula: C23H19N3O2
• Molecular Weight: 369.423
• DSSTox Substance ID: DTXSID80450266
• Nikkaji Number: J656.955B

Synonyms:142719-61-7;4'-(3,4-Dimethoxyphenyl)-2,2':6',2''-terpyridine;2,2':6',2''-Terpyridine, 4'-(3,4-dimethoxyphenyl)-;SCHEMBL16576443;DTXSID80450266

Chemical Property of 2,2':6',2''-Terpyridine, 4'-(3,4-dimethoxyphenyl)-

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 369.147726857
• Heavy Atom Count: 28
• Complexity: 451

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1)C2=CC(=NC(=C2)C3=CC=CC=N3)C4=CC=CC=N4)OC

Technology Process of 2,2':6',2''-Terpyridine, 4'-(3,4-dimethoxyphenyl)-

There total 1 articles about 2,2':6',2''-Terpyridine, 4'-(3,4-dimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

3-(3,4-dimethoxyphenyl)-1-(pyridin-2-yl)prop-2-en-1-one (92963-55-8) + 1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide (26482-00-8) → 4′-(3,4-dimethoxyphenyl)-2,2′:6′,2″-terpyridine (142719-61-7)

Guidance literature:

With ammonium acetate; In acetic acid; Heating;

Reference yield: 98.2%

copper(II) choride dihydrate + 4′-(3,4-dimethoxyphenyl)-2,2′:6′,2″-terpyridine (142719-61-7) + Naprelan (26159-34-2) → [Cu(4'-(3,4-dimethoxyphenyl)-2,2':6',2''-terpyridine)(nap)Cl]

Guidance literature:

In methanol; at 20 ℃; for 4h; Reflux;

DOI:10.1039/c5nj01059d

Reference yield: 93.1%

copper(II) choride dihydrate + 4′-(3,4-dimethoxyphenyl)-2,2′:6′,2″-terpyridine (142719-61-7) → [copper(II)(4′-(3,4-dimethoxyphenyl)-2,2′:6′,2″-terpyridine)2](chloride)2

Guidance literature:

In methanol; for 2h; Reflux;

DOI:10.1039/c5dt03831f

upstream raw materials:

3-(3,4-dimethoxyphenyl)-1-(pyridin-2-yl)prop-2-en-1-one

1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide

Downstream raw materials:

Os(4'-(3,4-dimethoxyphenyl)-2,2':6',2''-terpyridine)2⁽²⁺⁾

Fe(4'-(3,4-dimethoxyphenyl)-2,2':6',2''-terpyridine)2⁽²⁺⁾

Co(4'-(3,4-dimethoxyphenyl)-2,2':6',2''-terpyridine)2⁽²⁺⁾

Ni(4'-(3,4-dimethoxyphenyl)-2,2':6',2''-terpyridine)2⁽²⁺⁾

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