Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)-

Base Information

Chemical Name:Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)-
CAS No.:14326-08-0
Molecular Formula:C22H20O4
Molecular Weight:348.398
Hs Code.:
DSSTox Substance ID:DTXSID10471944
Nikkaji Number:J2.744.558F
Wikidata:Q82300649

Synonyms:Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)-;14326-08-0;SCHEMBL6444060;DTXSID10471944

Suppliers and Price of Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)-

Chemical Property:

Melting Point:156-158 °C
Boiling Point:217-220 °C(Press: 0.2 Torr)
PSA：44.76000
Density:1.182±0.06 g/cm3(Predicted)
LogP:4.66570
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:348.13615911
Heavy Atom Count:26
Complexity:401

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=CC(=C1)C=O)OCC2=CC=CC=C2)OCC3=CC=CC=C3

Technology Process of Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)-

There total 6 articles about Benzaldehyde, 3-methoxy-4,5-bis(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3934-87-0
5-hydroxyvanillin

: 100-39-0
benzyl bromide

: 14326-08-0
3,4-bis(benzyloxy)-5-methoxybenzaldehyde

Guidance literature:: With potassium carbonate; In acetone; for 7h; Reflux;
DOI:10.1021/ja9039407

Reference yield: 100.0%

: 82628-68-0
3,4-dihydroxy-5-methylbenzaldehyde

: 100-39-0
benzyl bromide

: 14326-08-0
3,4-bis(benzyloxy)-5-methoxybenzaldehyde

Guidance literature:: 3,4-dihydroxy-5-methylbenzaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; for 0.5h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide;
DOI:10.1002/cbdv.200800224

Reference yield:

: 5438-36-8
5-iodovaniline

: 14326-08-0
3,4-bis(benzyloxy)-5-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH; CuSO₄ / 6 h / 125 °C

2: K₂CO₃ / dimethylformamide / 4 h / 70 °C

With sodium hydroxide; potassium carbonate; copper(II) sulfate; In N,N-dimethyl-formamide;
DOI:10.1039/b304411d