3,4-Dihydroxy-5-methylbenzaldehyde

Base Information

Chemical Name:3,4-Dihydroxy-5-methylbenzaldehyde
CAS No.:82628-68-0
Molecular Formula:C8H8O3
Molecular Weight:152.15
Hs Code.:
DSSTox Substance ID:DTXSID70457860
Wikidata:Q82280892

Synonyms:3,4-dihydroxy-5-methylbenzaldehyde;82628-68-0;3,4-dihydroxy-5-methyl-benzaldehyde;SCHEMBL299751;DTXSID70457860

Suppliers and Price of 3,4-Dihydroxy-5-methylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3,4-Dihydroxy-5-methylbenzaldehyde

Chemical Property:

XLogP3:0.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:152.047344113
Heavy Atom Count:11
Complexity:146

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=CC(=C1O)O)C=O

Technology Process of 3,4-Dihydroxy-5-methylbenzaldehyde

There total 5 articles about 3,4-Dihydroxy-5-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 32263-14-2
4-hydroxy-3-methoxy-5-methylbenzaldehyde

: 82628-68-0
3,4-dihydroxy-5-methylbenzaldehyde

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃;

Reference yield:

: 87743-10-0
3-((dimethylamino)methyl)-4-hydroxy-5-methoxybenzaldehyde

: 82628-68-0
3,4-dihydroxy-5-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 24 h / Reflux

1.2: 2 h / 20 °C

1.3: 0.75 h / Reflux

2.1: boron tribromide / dichloromethane / 0 - 20 °C

With acetic anhydride; boron tribromide; In dichloromethane;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 82628-68-0
3,4-dihydroxy-5-methylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; ethanol / 20 °C / Reflux

2.1: acetic anhydride / 24 h / Reflux

2.2: 2 h / 20 °C

2.3: 0.75 h / Reflux

3.1: boron tribromide / dichloromethane / 0 - 20 °C

With acetic anhydride; boron tribromide; In ethanol; dichloromethane; water;