4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5

Base Information

Chemical Name:4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5
CAS No.:871810-44-5
Molecular Formula:C₂₈H₃₂N₂O₇S
Molecular Weight:540.637
Hs Code.:

Synonyms:

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Chemical Property of 4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5

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Technology Process of 4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5

There total 1 articles about 4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6590-65-4
N-(2-Formyl-phenyl)-4-methyl-benzenesulfonamide

: 60835-71-4
4'-aminobenzo-15-crown-5-ether

: 871810-44-5
4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5

Guidance literature:: In benzene; for 2h; Heating;
DOI:10.1107/S0108768107003898

Reference yield:

: 871810-44-5
4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5

: 2(lithium perchlorate)*[Cu(N-(4-benzo-15-crown-5)-2-(amino-N-tosyl)phenylaldiminate)2]*2H₂O

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: acetonitrile

In methanol; acetonitrile;
DOI:10.1134/S0036023608060120

Reference yield:

: 871810-44-5
4'-[2-(tosylamino)benzylideneamino]-2,3-benzo-15-crown-5

: 557-34-6
zinc diacetate

: 916676-16-9
bis[N-(4'-benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine]zinc

Guidance literature:: In methanol; Zn salt added to ligand in CH3OH, refluxed for 2 h; filtered, recrystd.(alcohol), elem. anal.;
DOI:10.1134/S107032840603002X