Technology Process of Phosphonic diamide, N,N,N',N'-tetramethyl-P-(phenylmethyl)-
There total 14 articles about Phosphonic diamide, N,N,N',N'-tetramethyl-P-(phenylmethyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
Heating;
- Guidance literature:
-
pentamethylphosphonic diamide;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.5h;
With
copper(l) iodide;
In
tetrahydrofuran; hexane;
at -40 - -30 ℃;
for 1h;
iodobenzene;
palladium diacetate; 1,2-bis-(diphenylphosphino)ethane;
In
tetrahydrofuran; hexane;
for 6h;
Heating;
- Guidance literature:
-
With
triethylamine;
In
diethyl ether;
for 6h;
Ambient temperature;
DOI:10.1021/ja00085a026