7-Phenyl-1,4,7-dithiaphosphonane

Base Information

Chemical Name:7-Phenyl-1,4,7-dithiaphosphonane
CAS No.:146719-81-5
Molecular Formula:C₁₂H₁₇PS₂
Molecular Weight:256.373
Hs Code.:
DSSTox Substance ID:DTXSID10571150
Nikkaji Number:J1.190.421A
Wikidata:Q82458776
Mol file:146719-81-5.mol

Synonyms:7-Phenyl-1,4,7-dithiaphosphonane;146719-81-5;1-Phenyl-1-phospha-4,7-dithiacyclononane;SCHEMBL9370155;DTXSID10571150

Suppliers and Price of 7-Phenyl-1,4,7-dithiaphosphonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 7-Phenyl-1,4,7-dithiaphosphonane

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:256.05092989
Heavy Atom Count:15
Complexity:159

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CSCCSCCP1C2=CC=CC=C2

Technology Process of 7-Phenyl-1,4,7-dithiaphosphonane

There total 1 articles about 7-Phenyl-1,4,7-dithiaphosphonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3190-78-1
3-phenyl-3-phosphapentane-1,5-dithiol

: 107-06-2,52399-93-6
1,2-dichloro-ethane

: 146719-81-5
1-phenyl-1-phospha-4,7-dithiacyclononane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 22h;
DOI:10.1039/c39930000054

Reference yield: 88.0%

: iron(II) tetrafluoroborate

: 146719-81-5
1-phenyl-1-phospha-4,7-dithiacyclononane

: [Co(1-phenyl-1-phospha-4,7-dithiacyclononane)2][BF₄]2

Guidance literature:: In acetonitrile; N2-atmosphere; stirring for 15 min; pptn. on Et2O addn., collection (filtration), drying (vac.); elem. anal.;
DOI:10.1016/S0020-1693(99)00206-6

Reference yield: 80.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 146719-81-5
1-phenyl-1-phospha-4,7-dithiacyclononane

: 147105-55-3
[Cu(η(1)-1-phenyl-1-phospha-4,7-dithiacyclononane)(η(3)-1-phenyl-1-phospha-4,7-dithiacyclononane)][PF6]

Guidance literature:: In acetonitrile; N2-atmosphere; excess ligand, stirring for 5 min; Et2O addn., crystn. (4°C, overnight), collection (filtration), drying (vac.); elem. anal.;
DOI:10.1016/S0020-1693(99)00206-6