11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide

Base Information

• Chemical Name: 11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide
• CAS No.: 122048-34-4
• Molecular Formula: C₂₅H₂₂O₂
• Molecular Weight: 354.448

Synonyms:

Chemical Property of 11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide

Chemical Property:

Purity/Quality:

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Technology Process of 11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide

There total 2 articles about 11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

13,14-dihydrobenzochrysene (122048-29-7) + 3-chloro-benzenecarboperoxoic acid (937-14-4) → 11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide (122048-34-4) + trans-11,12-dihydroxy-11,12,13,14-tetrahydrobenzochrysene (122048-32-2,122048-33-3,122090-51-1,122090-52-2) + 3-Chloro-benzoic acid 12-hydroxy-11,12,13,14-tetrahydro-benzo[g]chrysen-11-yl ester (122048-31-1,122048-43-5)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00276a009

Reference yield:

13,14-dihydrobenzochrysene (122048-29-7) + acetone (67-64-1) → 11,12,13,14-tetrahydrobenzochrysene 11,12-acetonide (122048-34-4) + trans-11,12-dihydroxy-11,12,13,14-tetrahydrobenzochrysene (122048-32-2,122048-33-3,122090-51-1,122090-52-2) + 3-Chloro-benzoic acid 12-hydroxy-11,12,13,14-tetrahydro-benzo[g]chrysen-11-yl ester (122048-31-1,122048-43-5)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00276a009

upstream raw materials:

13,14-dihydrobenzochrysene

3-chloro-benzenecarboperoxoic acid

acetone

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