Fluorodiiodomethane

Base Information

• Chemical Name: Fluorodiiodomethane
• CAS No.: 1493-01-2
• Molecular Formula: CHFI2
• Molecular Weight: 285.826
• Mol file: 1493-01-2.mol

Synonyms:diiodofluoro methane;Methane, fluorodiiodo-;fluoro-diiodo-methane;Fluordiiodmethan;Methane,fluorodiiodo;Fluor-dijod-methan;

Chemical Property of Fluorodiiodomethane

Chemical Property:

• Vapor Pressure: 10.2mmHg at 25°C
• Melting Point: -35--31℃
• Boiling Point: 134oC at 760 mmHg
• Flash Point: 43.4oC
• PSA: 0.00000
• Density: 3.229g/cm3
• LogP: 2.10950

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Fluorodiiodomethane

There total 1 articles about Fluorodiiodomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iodoform (75-47-8) → trifluoromethan (75-46-7) + iododifluoromethane (1493-03-4) + fluorodiiodomethane (1493-01-2)

Guidance literature:

at 80 ℃;

Reference yield: 88.0%

fluorodiiodomethane (1493-01-2) + benzyl N-<(R)-1-phenylethyl>-N-vinylcarbamate (152615-27-5) → benzyl N-<(1R*,2R*)-2-fluorocyclopropyl>-N-<(R)-1-phenylethyl>carbamate + benzyl N-<(1R*,2S*)-2-fluorocyclopropyl>-N-<(R)-1-phenylethyl>carbamate

Guidance literature:

With diethylzinc; In hexane; dichloromethane; at -40 ℃; for 0.5h;

DOI:10.1016/S0040-4020(01)89665-4

Reference yield: 87.0%

fluorodiiodomethane (1493-01-2) + benzyl N-(1-phenylethyl)-N-vinylcarbamate (142977-33-1) → benzyl N-<(1R*,2R*)-2-fluorocyclopropyl>-N-(1-phenylethyl)carbamate (142977-39-7,151123-40-9,151123-41-0,151123-42-1,151123-43-2) + benzyl N-<(1R*,2S*)-2-fluorocyclopropyl>-N-(1-phenylethyl)carbamate (142977-39-7,151123-40-9,151123-41-0,151123-42-1,151123-43-2)

Guidance literature:

With diethylzinc; In hexane; dichloromethane; at -40 ℃; for 0.5h;

DOI:10.1016/S0040-4020(01)89665-4

upstream raw materials:

iodoform

Downstream raw materials:

iodoform

(2-Fluorocyclopropyl)benzene

(fluoromethyl)triphenylphosphonium iodide

fluoroiodomethyltriphenylphosphonium iodide