1,3-Butanedione, 1-(3-bromophenyl)-

Base Information

Chemical Name:1,3-Butanedione, 1-(3-bromophenyl)-
CAS No.:152706-83-7
Molecular Formula:C10H9BrO2
Molecular Weight:241.084
Hs Code.:

Synonyms:(3-bromobenzoyl)acetone;1-(3-Bromophenyl)butane-1,3-dione;1-(3-Bromophenyl)-1,3-butanedione;3-bromobenzoylacetone;m-Brom-benzoylaceton;

Suppliers and Price of 1,3-Butanedione, 1-(3-bromophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(3-BROMOPHENYL)BUTANE-1,3-DIONE 95.00%
5MG
$ 496.25

Acrotein
1-(3-Bromophenyl)-1,3-butanedione 97%
0.5g
$ 121.00

ACHEMBLOCK
1-(3-Bromophenyl)-1,3-butanedione 95%
5G
$ 660.00

ACHEMBLOCK
1-(3-Bromophenyl)-1,3-butanedione 95%
1G
$ 220.00

Total 6 raw suppliers

Chemical Property of 1,3-Butanedione, 1-(3-bromophenyl)-

Chemical Property:

Melting Point:15-43 °C
Boiling Point:327.4±22.0 °C(Predicted)
PSA：34.14000
Density:1.441±0.06 g/cm3(Predicted)
LogP:2.61090

Purity/Quality:

123% ^*data from raw suppliers

1-(3-BROMOPHENYL)BUTANE-1,3-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Butanedione, 1-(3-bromophenyl)-

There total 2 articles about 1,3-Butanedione, 1-(3-bromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 141-78-6
ethyl acetate

: 2142-63-4
1-(3-Bromophenyl)ethanone

: 152706-83-7
1-(3-bromophenyl)butane-1,3-dione

Guidance literature:: ethyl acetate; With ethanol; sodium hydride; In tetrahydrofuran; Cooling with ice;

1-(3-Bromophenyl)ethanone; In tetrahydrofuran; at 20 ℃;

With 18-crown-6 ether; In tetrahydrofuran; at 20 ℃; Reflux;
DOI:10.1021/acs.jmedchem.6b00829

Reference yield:

: 24398-88-7
ethyl 3-bromobenzoate

: 67-64-1
acetone

: 152706-83-7
1-(3-bromophenyl)butane-1,3-dione

Guidance literature:: With sodium hydride; In diethyl ether;
DOI:10.1055/s-0029-1217373

Reference yield: 89.0%

: 152706-83-7
1-(3-bromophenyl)butane-1,3-dione

: 14337-43-0
ethyl 2-chloro-2-(hydroxyimino)acetate

: 1229442-24-3
ethyl 4-(3-bromobenzoyl)-5-methylisoxazole-3-carboxylate

Guidance literature:: 1-(3-bromophenyl)butane-1,3-dione; With sodium; In ethanol; at 0 ℃; for 0.25h;

ethyl 2-chloro-2-(hydroxyimino)acetate; In ethanol; at 0 - 20 ℃; regioselective reaction;
DOI:10.1021/acs.jmedchem.6b00829