(Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine

Base Information

Chemical Name:(Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine
CAS No.:153358-06-6
Molecular Formula:C20H18NP
Molecular Weight:303.343
Hs Code.:
DSSTox Substance ID:DTXSID60572672
Nikkaji Number:J1.021.597H
Mol file:153358-06-6.mol

Synonyms:153358-06-6;SCHEMBL10309892;(Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine;DTXSID60572672

Suppliers and Price of (Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:303.117686576
Heavy Atom Count:22
Complexity:324

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN=CC1=CC=CC=C1P(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of (Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine

There total 1 articles about (Z)-1-[2-(Diphenylphosphanyl)phenyl]-N-methylmethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 50777-76-9
(2-formylphenyl)(diphenyl)phosphine

: 74-89-5
methylamine

: 153358-06-6
N-[2-(diphenylphosphanyl)benzylidene]-N-methylamine

Guidance literature:: In tetrahydrofuran; methanol; 1.) 0 deg C, 1 h, 2.) to 15 deg C;

Reference yield: 95.0%

: 153358-06-6
N-[2-(diphenylphosphanyl)benzylidene]-N-methylamine

: 127171-70-4
N-(2-(diphenylphosphino)benzyl)-N-methylamine

Guidance literature:: With sodium tetrahydroborate; methylamine; In tetrahydrofuran; methanol; at 0 ℃;

Reference yield: 94.0%

: 591-50-4
iodobenzene

: 153358-06-6
N-[2-(diphenylphosphanyl)benzylidene]-N-methylamine

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 217813-25-7
Pd(phenyl)I(N-[2-(diphenylphosphanyl)benzylidene]-N-methylamine)

Guidance literature:: In tetrahydrofuran; byproducts: dibenzylideneacetone, Pd; N2 atmosphere, addn. of phosphanyl-amine ligand and PhI to soln. of Pd complex at 50°C, stirring (50°C, 45 min); concn., filtration, removement of solvent (reduced pressure), washing (Et2O), drying (vacuum); elem. anal.;
DOI:10.1002/(sici)1099-0682(199811)1998:11<1811::aid-ejic1811>3.0.co;2-r