[μ-7-nitro-1,3,5-triazaadamantane-κN¹:κN³]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN⁴]diplatinum

Base Information

• Chemical Name: [μ-7-nitro-1,3,5-triazaadamantane-κN¹:κN³]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN⁴]diplatinum
• CAS No.: 1247794-14-4
• Molecular Formula: C₃₉H₄₄Cl₄N₈O₆Pt₂
• Molecular Weight: 1252.8

Synonyms:

Chemical Property of [μ-7-nitro-1,3,5-triazaadamantane-κN¹:κN³]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN⁴]diplatinum

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [μ-7-nitro-1,3,5-triazaadamantane-κN¹:κN³]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN⁴]diplatinum

There total 4 articles about [μ-7-nitro-1,3,5-triazaadamantane-κN¹:κN³]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN⁴]diplatinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

trans-(benzonitrile)-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum (1247793-74-3) + 7-nitro-1,3,5-triazaadamantane (14612-28-3) → trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][7-nitro-1,3,5-triazaadamantane-κN(1)]platinum (1247793-93-6) + [μ-7-nitro-1,3,5-triazaadamantane-κN1:κN3]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN4]diplatinum (1247794-14-4)

Guidance literature:

In chloroform; soln. Pt complex and 7-nitro-1,3,5-triaza-adamantane in CHCl3 was stirred at room temp. for 2 weeks; solvent was evapd., product was purified by chromy. on silica (CH2Cl2-Et2O 98:2); elem. anal.;

DOI:10.1039/c0dt00360c

Reference yield:

trans-bis(benzonitrile)dichloroplatinum(II) (14873-63-3,15617-19-3,51921-56-3) → trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][7-nitro-1,3,5-triazaadamantane-κN(1)]platinum (1247793-93-6) + [μ-7-nitro-1,3,5-triazaadamantane-κN1:κN3]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN4]diplatinum (1247794-14-4)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform

2: chloroform

In chloroform;

DOI:10.1039/c0dt00360c

Reference yield:

N-(2-methoxybenzylidene)methanamine N-oxide (33499-30-8) → trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][7-nitro-1,3,5-triazaadamantane-κN(1)]platinum (1247793-93-6) + [μ-7-nitro-1,3,5-triazaadamantane-κN1:κN3]tetrachlorobis[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN4]diplatinum (1247794-14-4)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform

2: chloroform

In chloroform;

DOI:10.1039/c0dt00360c

upstream raw materials:

trans-(benzonitrile)-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum

7-nitro-1,3,5-triazaadamantane

N-(2-methoxybenzylidene)methanamine N-oxide

trans-bis(benzonitrile)dichloroplatinum(II)

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