N-(2-Bromophenyl)-N-methylacetamide

Base Information

Chemical Name:N-(2-Bromophenyl)-N-methylacetamide
CAS No.:153704-11-1
Molecular Formula:C9H10BrNO
Molecular Weight:228.088
Hs Code.:
DSSTox Substance ID:DTXSID101293368
Nikkaji Number:J1.009.384H
Mol file:153704-11-1.mol

Synonyms:153704-11-1;Acetamide, N-(2-bromophenyl)-N-methyl-;N-(2-Bromophenyl)-N-methylacetamide;SCHEMBL9062523;DTXSID101293368;Acetamide,N-(2-bromophenyl)-N-methyl-;CID 11031599;F53216

Suppliers and Price of N-(2-Bromophenyl)-N-methylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N-(2-Bromophenyl)-N-methylacetamide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:226.99458
Heavy Atom Count:12
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N(C)C1=CC=CC=C1Br

Technology Process of N-(2-Bromophenyl)-N-methylacetamide

There total 9 articles about N-(2-Bromophenyl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 698-00-0
2-bromo-N,N-dimethylaniline

: 108-24-7
acetic anhydride

: 153704-11-1
N-(2-bromophenyl)-N-methylacetamide

Guidance literature:: With oxygen; copper diacetate; In acetonitrile; for 36h; Schlenk technique; Sealed tube; Reflux;
DOI:10.1039/c5cc07454a

Reference yield: 79.0%

: 614-76-6
N-acetyl-2-bromoaniline

: 74-88-4
methyl iodide

: 153704-11-1
N-(2-bromophenyl)-N-methylacetamide

Guidance literature:: N-acetyl-2-bromoaniline; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jacs.1c12043

Reference yield: 72.0%

: 579-10-2
N-acetyl-N-methylaniline

: 153704-11-1
N-(2-bromophenyl)-N-methylacetamide

Guidance literature:: With N-Bromosuccinimide; cobalt acetylacetonate; trifluoroacetic acid; silver(l) oxide; In 1,2-dichloro-ethane; at 60 ℃; for 16h; regioselective reaction;
DOI:10.1039/c8ob01448e