(η5-cyclopentadienyl)(η3-1-methylallyl)(triphenylphosphine)iron

Base Information

Chemical Name:(η5-cyclopentadienyl)(η3-1-methylallyl)(triphenylphosphine)iron
CAS No.:110221-09-5
Molecular Formula:C₂₇H₂₇FeP
Molecular Weight:438.332
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η5-cyclopentadienyl)(η3-1-methylallyl)(triphenylphosphine)iron

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Technology Process of (η5-cyclopentadienyl)(η3-1-methylallyl)(triphenylphosphine)iron

There total 1 articles about (η5-cyclopentadienyl)(η3-1-methylallyl)(triphenylphosphine)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 19543-98-7
bis(triphenylphosphine)iron(II) chloride

: 74-85-1
ethene

: 16733-97-4
cyclopentadienyllithium

: 3536-96-7
vinylmagnesium chloride

: 110221-09-5
(η5-cyclopentadienyl)(η3-1-methylallyl)(triphenylphosphine)iron

Guidance literature:: In tetrahydrofuran; diethyl ether; standing of the iron-complex, CpLi and an ethereal soln. of the Grignard-compd. in THF satd. with ethylene for 24 h at -80°C (under Ar),warming to -40°C, warming of soln. to room temp. (C2H4-pressure:20 bar); removal of solvent in vac., addn. of toluene to residue, filtration, addn. of pentane to filtrate, filtration, removal of solvents, dissolving residue (toluene), addn. of pentane, filtration, standing of filtrate at-20°C (crystn.);