Benzene, 1-(2,2-difluoroethenyl)-4-methoxy-

Base Information

Chemical Name:Benzene, 1-(2,2-difluoroethenyl)-4-methoxy-
CAS No.:1608-24-8
Molecular Formula:C9H8F2O
Molecular Weight:170.159
Hs Code.:
DSSTox Substance ID:DTXSID30454198
Nikkaji Number:J681.444A

Synonyms:Benzene, 1-(2,2-difluoroethenyl)-4-methoxy-;1608-24-8;1-(2,2-Difluorovinyl)-4-methoxybenzene;1-(2,2-difluoroethenyl)-4-methoxybenzene;SCHEMBL10049316;DTXSID30454198;TUSNPYTWRBGHSW-UHFFFAOYSA-N;4-methoxy-beta,beta-difluorostyrene;beta,beta-Difluoro-4-methoxystyrene;CS-0530888;EN300-6492056

Suppliers and Price of Benzene, 1-(2,2-difluoroethenyl)-4-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Benzene, 1-(2,2-difluoroethenyl)-4-methoxy-

Chemical Property:

PSA：9.23000
LogP:2.93260
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:170.05432120
Heavy Atom Count:12
Complexity:156

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=C(F)F

Technology Process of Benzene, 1-(2,2-difluoroethenyl)-4-methoxy-

There total 26 articles about Benzene, 1-(2,2-difluoroethenyl)-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 2236129-81-8
trifluoroacetaldehyde N-triftosylhydrazone

: 1608-24-8
3-(2,2-difluoroethenyl)anisole

Guidance literature:: With ammonium chloride; lithium hydroxide; at 100 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b03740

Reference yield: 87.0%

: 696-62-8
para-iodoanisole

: 2,2-difluorovinylzinc chloride N,N,N',N'-tetramethylethylenediamine

: 1608-24-8
3-(2,2-difluoroethenyl)anisole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; for 6h; Reflux;
DOI:10.1246/cl.2011.986

Reference yield: 87.0%

: 696-62-8
para-iodoanisole

: 101032-99-9
2,2-difluorovinylzinc chloride

: 1608-24-8
3-(2,2-difluoroethenyl)anisole

Guidance literature:: With sulfuric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1016/0022-328X(87)80001-3