N,N-Dimethyl-2-furan-1-propanamine

Base Information

• Chemical Name: N,N-Dimethyl-2-furan-1-propanamine
• CAS No.: 25435-32-9
• Molecular Formula: C₉H₁₅NO
• Molecular Weight: 153.224
• Hs Code.: 2932190090
• Mol file: 25435-32-9.mol

Synonyms:2-Furanpropylamine,N,N-dimethyl- (8CI)

Chemical Property of N,N-Dimethyl-2-furan-1-propanamine

Chemical Property:

• Vapor Pressure: 0.436mmHg at 25°C
• Boiling Point: 194.7°C at 760 mmHg
• Flash Point: 71.5°C
• PSA: 16.38000
• Density: 0.946g/cm³
• LogP: 1.77380

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-Dimethyl-2-furan-1-propanamine

There total 4 articles about N,N-Dimethyl-2-furan-1-propanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-(2-furyl)propionaldehyde (4543-51-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 1-(2-furyl)-3-dimethylaminopropane (25435-32-9)

Guidance literature:

With TiO₂-350; In water; for 12h; under 750.075 Torr; Inert atmosphere; Irradiation;

Reference yield: 65.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N,N,N-tris<1-(2-furyl)propyl>perhydro-1,3,5-triazine (86043-42-7) → 1-(2-furyl)-3-dimethylaminopropane (25435-32-9)

Guidance literature:

With hydrogen; nickel; In ethanol; water; at 30 ℃;

DOI:10.1007/BF00506419

Reference yield:

3-(2-furyl)-1-chloropropane (40517-25-7) + dimethyl amine (124-40-3) → 1-(2-furyl)-3-dimethylaminopropane (25435-32-9)

Guidance literature:

at 120 ℃;

upstream raw materials:

3-(2-furyl)-1-chloropropane

dimethyl amine

formaldehyd

N,N,N-tris<1-(2-furyl)propyl>perhydro-1,3,5-triazine

Downstream raw materials:

(3-[2]furyl-propyl)-trimethyl-ammonium; iodide

ethyl-(3-[2]furyl-propyl)-dimethyl-ammonium; iodide

Refernces

• 1、 Buntyakova, N. A.,Taraskin, K. A.,Kharchenko, V. G.. "FORMATION OF N,N,N-TRIFURYLALKYLPERHYDRO-1,3,5-TRIAZINES IN THE REDUCTIVE ALKYLATION OF PRIMARY FURAN AMINES WITH FORMALDEHYDE". . p. 142 - 144. Retrieved 2007/10/02.