Methyl 5-Benzyloxy-4-Methoxy-2-nitrobenzoate

Base Information

• Chemical Name: Methyl 5-Benzyloxy-4-Methoxy-2-nitrobenzoate
• CAS No.: 164161-49-3
• Molecular Formula: C16H15NO6
• Molecular Weight: 317.298
• Hs Code.: 2918990090
• Mol file: 164161-49-3.mol

Synonyms:methyl 5-(benzyloxy)-4-methoxy-2-nitrobenzoate;4-methoxy-2-nitro-5-(phenylmethoxy)-benzoic acid,methyl ester;Methyl 5-benzyloxy-4-methoxy-2-nitrobenzoate;

Chemical Property of Methyl 5-Benzyloxy-4-Methoxy-2-nitrobenzoate

Chemical Property:

• Boiling Point: 482.4±40.0 °C(Predicted)
• PSA: 90.58000
• Density: 1.280
• LogP: 3.49220
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

Methyl 5-benzyloxy-4-methoxy-2-nitrobenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 5-Benzyloxy-4-Methoxy-2-nitrobenzoate

There total 11 articles about Methyl 5-Benzyloxy-4-Methoxy-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methyl 5-hydroxy-4-methoxy-2-nitrobenzoate (215659-03-3) + benzyl bromide (100-39-0) → methyl 5-(benzyloxy)-4-methoxy-2-nitrobenzoate (164161-49-3)

Guidance literature:

With potassium carbonate; In acetonitrile; at 80 ℃; for 4h;

Reference yield: 96.0%

3-hydroxy-4-methoxybenzoate (6702-50-7) + benzyl bromide (100-39-0) → methyl 5-(benzyloxy)-4-methoxy-2-nitrobenzoate (164161-49-3)

Guidance literature:

With nitric acid; potassium carbonate; acetic acid; sodium sulfate; In water; N,N-dimethyl-formamide;

Reference yield: 94.0%

→ methyl 5-(benzyloxy)-4-methoxy-2-nitrobenzoate (164161-49-3)

Guidance literature:

upstream raw materials:

methyl 5-hydroxy-4-methoxy-2-nitrobenzoate

benzyl bromide

methyl 3-(benzyloxy)-4-methoxy-benzoate

3-hydroxy-4-methoxybenzoate

Downstream raw materials:

6-(benzyloxy)-7-methoxyquinazolin-4(3H)-one

methyl 2-amino-5-hydroxy-4-methoxybenzoate

benzyl 2-amino-5-(benzyloxy)-4-methoxybenzoic acid

7-methoxy-4-pyridin-3-yl-6-(2-quinolin-2-ylethoxy)quinazoline

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