Technology Process of Octane, 1,1'-[methylenebis(oxy)]bis-
There total 5 articles about Octane, 1,1'-[methylenebis(oxy)]bis- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,4-Dichloro-6-methoxy-1,3,5-triazine;
In
toluene;
at 80 ℃;
for 4h;
DOI:10.1055/s-0029-1216992
- Guidance literature:
-
With
iron(III) chloride;
In
dichloromethane;
for 2h;
Product distribution;
Ambient temperature;
other reaction time; other temperature, solvent;
DOI:10.1021/jo970509l
- Guidance literature:
-
octanol;
With
aluminium(III) triflate; [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylene methane)];
for 0.0833333h;
Inert atmosphere;
Schlenk technique;
carbon dioxide;
With
hydrogen;
at 80 ℃;
for 18h;
under 60006 Torr;
Catalytic behavior;
Schlenk technique;
Autoclave;
DOI:10.1002/anie.201606427