Carbamic acid, [(1S,2R)-3-[[(2-amino-6-benzothiazolyl)sulfonyl](2-methylpropyl)amino]- 2-hydroxy-1-(phenylmethyl)propyl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S,2R)-3-[[(2-amino-6-benzothiazolyl)sulfonyl](2-methylpropyl)amino]- 2-hydroxy-1-(phenylmethyl)propyl]-, phenylmethyl ester
CAS No.:169280-61-9
Molecular Formula:C29H34N4O5S2
Molecular Weight:582.745
Hs Code.:

Carbamic acid,
[(1S,2R)-3-[[(2-amino-6-benzothiazolyl)sulfonyl](2-methylpropyl)amino]-
2-hydroxy-1-(phenylmethyl)propyl]-, phenylmethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S,2R)-3-[[(2-amino-6-benzothiazolyl)sulfonyl](2-methylpropyl)amino]- 2-hydroxy-1-(phenylmethyl)propyl]-, phenylmethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [(1S,2R)-3-[[(2-amino-6-benzothiazolyl)sulfonyl](2-methylpropyl)amino]- 2-hydroxy-1-(phenylmethyl)propyl]-, phenylmethyl ester

There total 8 articles about Carbamic acid, [(1S,2R)-3-[[(2-amino-6-benzothiazolyl)sulfonyl](2-methylpropyl)amino]- 2-hydroxy-1-(phenylmethyl)propyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: carbamic acid, 2R-hydroxy-3-[[(4-aminophenyl)sulfonyl](2-methylpropyl)amino]-1S-(phenylmethyl)propyl-, phenylmethyl ester

: 333-20-0
potassium thioacyanate

: 169280-61-9
carbamic acid, 2R-hydroxy-3-[[(2-aminobenzothiazol-6-yl)sulfonyl](2-methylpropyl)amino]-1S-(phenylmethyl)propyl-, phenylmethyl ester

Guidance literature:: With copper(II) sulfate; In methanol; for 2h; Heating / reflux;

Reference yield: 54.0%

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 183554-21-4
3-S-amino-2R-hydroxy-1-[(2-aminobenzothiazol-6-sulfonyl)(2-methylpropyl)amino]-4-phenylbutane

: 169280-61-9
carbamic acid, 2R-hydroxy-3-[[(2-aminobenzothiazol-6-yl)sulfonyl](2-methylpropyl)amino]-1S-(phenylmethyl)propyl-, phenylmethyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.1016/j.bmc.2003.07.001

Reference yield:

: 183004-94-6
3-S-(N-tert-butyloxyformamido)-[2R-hydroxy-1-[(4-aminophenylsulfonyl)(2-methylpropyl)]amino]-4-phenylbutane

: 169280-61-9
carbamic acid, 2R-hydroxy-3-[[(2-aminobenzothiazol-6-yl)sulfonyl](2-methylpropyl)amino]-1S-(phenylmethyl)propyl-, phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / CuSO₄ / methanol / 2 h / Heating

2: 54 percent / Et₃N / dimethylformamide / 18 h / 20 °C

With copper(II) sulfate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2003.07.001