1,4-dimethyl-1H-indole-3-carbaldehyde

Base Information

• Chemical Name: 1,4-dimethyl-1H-indole-3-carbaldehyde
• CAS No.: 170489-16-4
• Molecular Formula: C₁₁H₁₁NO
• Molecular Weight: 173.214
• Hs Code.: 2933990090
• Mol file: 170489-16-4.mol

Synonyms:1,4-dimethylindole-3-carboxaldehyde;1,4-dimethyl-1H-indole-3-carbaldehyde;

Chemical Property of 1,4-dimethyl-1H-indole-3-carbaldehyde

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 334.131oC at 760 mmHg
• Flash Point: 155.877oC
• PSA: 22.00000
• Density: 1.09g/cm3
• LogP: 2.29920
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

1,4-dimethyl-1H-indole-3-carbaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-dimethyl-1H-indole-3-carbaldehyde

There total 7 articles about 1,4-dimethyl-1H-indole-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,4-dimethylindole (27816-52-0) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 1,4-dimethyl-1H-indole-3-carbaldehyde (170489-16-4)

Guidance literature:

With trichlorophosphate; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jacs.1c09889

Reference yield: 78.0%

1,4-dimethylindole (27816-52-0) + formaldehyd (50-00-0,30525-89-4,61233-19-0) → 1,4-dimethyl-1H-indole-3-carbaldehyde (170489-16-4)

Guidance literature:

With sodium benzoate; lithium perchlorate; 4-chloro-aniline; In water; acetonitrile; at 20 ℃; for 20h; Electrolysis;

DOI:10.1021/acs.orglett.9b02433

Reference yield: 70.0%

1,4-dimethylindole (27816-52-0) + trimethylamine (75-50-3) → 1,4-dimethyl-1H-indole-3-carbaldehyde (170489-16-4)

Guidance literature:

With tetrabutyl ammonium fluoride; water; at 80 ℃; for 24h; Electrolysis; Inert atmosphere; Green chemistry;

DOI:10.1039/d1gc00661d

upstream raw materials:

4-methyl-1H-indole-3-carboxaldehyde

methyl iodide

1,4-dimethylindole

N,N-dimethyl-formamide

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