Tm(benzohydroxamate)3

Base Information

Chemical Name:Tm(benzohydroxamate)3
CAS No.:89001-37-6
Molecular Formula:C₂₁H₁₈N₃O₆Tm
Molecular Weight:577.325
Hs Code.:

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Suppliers and Price of Tm(benzohydroxamate)3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tm(benzohydroxamate)3

Chemical Property:

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Technology Process of Tm(benzohydroxamate)3

There total 1 articles about Tm(benzohydroxamate)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13537-18-3
thulium(III) chloride

: 22513-32-2
acid sodium salt of benzohydroxamic acid

: 89001-37-6
Tm(benzohydroxamate)3

Guidance literature:: In water; reaction of TmCl3 and sodium hydrogen benzohydroxamate in an aq. soln.; filtering off the formed ppt., washing with water and drying in a vacuum desiccator over CaCl2 in the presence of P2O5, elem. anal.;

Reference yield:

: 66-71-7
1,10-Phenanthroline

: 89001-37-6
Tm(benzohydroxamate)3

: Tm(benzohydroxamate)3*3(1,10-phenanthroline)

Guidance literature:: In ethanol; chloroform; addn. of 1,10-phenanthroline to a soln. of Tm(benzohydroxamate)3 in ethanol/chloroform; evapn. of the soln. to half of its volume, addn. of 1 or 2 drops of an aq. soln. of dioxane and allowing the soln. to crystallize, collecting the crystals and drying in a vacuum desiccator over CaCl2 anc P2O5, elem. anal.;