dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)

Base Information

Chemical Name:dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)
CAS No.:81380-83-8
Molecular Formula:C₂₈H₂₂Cl₂P₂PtS₄
Molecular Weight:814.68
Hs Code.:

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Chemical Property of dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)

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Technology Process of dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)

There total 3 articles about dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 52379-41-6
2,2'-(phenylphosphiniden)bisthiophen

: 81380-83-8
dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)

Guidance literature:: In dichloromethane; to CH2Cl2 soln. of Pt-complex soln. of ligand in CH2Cl2 was added dropwise under N2, stirred at room temp. for 30 min; solvent was removed in vacuo, washed with hexane, recrystd. from CH2Cl2;

Reference yield:

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 52379-41-6
2,2'-(phenylphosphiniden)bisthiophen

: 81380-83-8
dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)

Guidance literature:: In dichloromethane; CH2Cl2 soln. of ligand was added dropwise to stirred soln. of Pt-complexin CH2Cl2, stirred for 45 min; solvent was removed in vacuo, washed with hexane, dissolved in CHCl3, passed through Florisil column with CHCl3, solvent was removed in vacuo, recrystd. from benzene; elem. anal.;

Reference yield:

: 10025-99-7
potassium tetrachloroplatinate(II)

: 52379-41-6
2,2'-(phenylphosphiniden)bisthiophen

: 81380-83-8
dichlorobis[phenyldi(2-thienyl)phosphine]platinum(II)

Guidance literature:: In ethanol; water; to hot soln. of phosphine in ethanol added dropwise cold soln. of K2PtCl4 in water, heated for 5 min, allowed to cool; elem. anal.;
DOI:10.1039/DT9820000051