Stannane, dichlorobis(4-fluorophenyl)-

Base Information

Chemical Name:Stannane, dichlorobis(4-fluorophenyl)-
CAS No.:17236-61-2
Molecular Formula:C12H8Cl2F2Sn
Molecular Weight:379.808
Hs Code.:
Mol file:17236-61-2.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, dichlorobis(4-fluorophenyl)-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Stannane, dichlorobis(4-fluorophenyl)-

There total 2 articles about Stannane, dichlorobis(4-fluorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1251-03-2
tetrakis(4-fluorophenyl)stannane

: 7646-78-8
tin(IV) chloride

: 17236-61-2
bis(4-fluorophenyl)tin dichloride

Guidance literature:: In neat (no solvent); slow heating of a mixt. of Sn-compd. and SnCl4 at 190°C for 2 h under N2, further heating at 205°C for 40 min; dissolution of resulting oil in hexane, removing slight turbidity by filtn., cooling to -78°C, filtn., rapidly washing with cold hexane, evapn. of mother liquor yields second crop, elem. anal.;
DOI:10.1016/0022-328X(94)80033-2

Reference yield: 68.0%

: 2250-97-7
bis[tri(p-fluorophenyl)tin]oxide

: 7647-18-9
antimonypentachloride

: C₁₂H₈F₂OSn

: 125689-47-6
bis-(4-fluoro-phenyl)-antimony ⁽³⁺⁾; tris chloride

: 17236-61-2
bis(4-fluorophenyl)tin dichloride

Guidance literature:: In diethyl ether; for 2h; Reflux;
DOI:10.14233/ajchem.2013.14969

Reference yield: 99.0%

: 3585-33-9
lithium dimethylamide

: 17236-61-2
bis(4-fluorophenyl)tin dichloride

: 952516-10-8
(p-FC₆H₄)2Sn(NMe₂)2

Guidance literature:: In benzene; under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;
DOI:10.1016/j.poly.2007.06.002