cis-{RuCl₂(CO)2(C₁₄H₂₃P)2}

Base Information

• Chemical Name: cis-{RuCl₂(CO)2(C₁₄H₂₃P)2}
• CAS No.: 20303-52-0
• Molecular Formula: C₃₀H₄₆Cl₂O₂P₂Ru
• Molecular Weight: 672.618
• Mol file: 20303-52-0.mol

Synonyms:

Chemical Property of cis-{RuCl₂(CO)2(C₁₄H₂₃P)2}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-{RuCl₂(CO)2(C₁₄H₂₃P)2}

There total 2 articles about cis-{RuCl₂(CO)2(C₁₄H₂₃P)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ruthenium(III) chloride trihydrate (14898-67-0) + carbon monoxide (201230-82-2) + (dibutyl)(phenyl)phosphine (6372-44-7) → trans-{RuCl2(CO)2(C14H23P)2} (20303-52-0)

Guidance literature:

In further solvent(s); passing CO through a boiling soln. of RuCl3*3H2O in 2-methoxyethanol; addn. of the phosphine to the hot soln.;; recrystn. from petroleum ether;;

Reference yield:

ruthenium(III) chloride trihydrate (14898-67-0) + carbon monoxide (201230-82-2) + (dibutyl)(phenyl)phosphine (6372-44-7) → cis-{RuCl2(CO)2(C14H23P)2} (20303-52-0)

Guidance literature:

In further solvent(s); treating a boiling soln. of RuCl3*3H2O with CO; addn. of the phosphine;; recrystn. from petroleum ether;;

Reference yield:

cis-{RuCl2(CO)2(C14H23P)2} (20303-52-0) + lithium bromide (7550-35-8) → cis-{RuBr2(CO)2(C14H23P)2} (21199-64-4)

Guidance literature:

In further solvent(s); boiling the soln. of the dichloro-compound in 2-methoxyethanol with LiBr;; recrystn.;;

upstream raw materials:

ruthenium(III) chloride trihydrate

carbon monoxide

(dibutyl)(phenyl)phosphine

Downstream raw materials:

cis-{RuBr₂(CO)2(C₁₄H₂₃P)2}