Benzenepentanamide, b-hydroxy-N-methoxy-N-methyl-

Base Information

Chemical Name:Benzenepentanamide, b-hydroxy-N-methoxy-N-methyl-
CAS No.:176536-24-6
Molecular Formula:C13H19NO3
Molecular Weight:237.299
Hs Code.:

Synonyms:

Suppliers and Price of Benzenepentanamide, b-hydroxy-N-methoxy-N-methyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepentanamide, b-hydroxy-N-methoxy-N-methyl-

Chemical Property:

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Technology Process of Benzenepentanamide, b-hydroxy-N-methoxy-N-methyl-

There total 5 articles about Benzenepentanamide, b-hydroxy-N-methoxy-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 21080-41-1,41479-99-6
β-hydroxy-benzenepentanoic acid

: 1117-97-1
N,0-dimethylhydroxylamine

: 176536-24-6
3-hydroxy-N-methoxy-N-methyl-5-phenylpentanamide

Guidance literature:: With C₁₂H₆B₂Br₄O₃; In 1,2-dichloro-ethane; at 90 ℃; for 24h;
DOI:10.1039/d0cc05630h

Reference yield: 77.0%

: 53376-62-8
ethyl 3-hydroxy-5-phenylpentanoate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 176536-24-6
3-hydroxy-N-methoxy-N-methyl-5-phenylpentanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In tetrahydrofuran; toluene; at 0 - 20 ℃; Inert atmosphere;

ethyl 3-hydroxy-5-phenylpentanoate; In tetrahydrofuran; toluene; at -40 - 20 ℃; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; toluene;
DOI:10.1002/anie.200802162

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 78191-00-1
N-Methoxy-N-methylacetamide

: 176536-24-6
3-hydroxy-N-methoxy-N-methyl-5-phenylpentanamide

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, -78 deg C;
DOI:10.1021/ja953901u