2,3-Epoxypropyl methanesulphonate

Base Information

• Chemical Name: 2,3-Epoxypropyl methanesulphonate
• CAS No.: 6177-60-2
• Molecular Formula: C4H8 O4 S
• Molecular Weight: 152.171
• European Community (EC) Number: 228-223-0
• DSSTox Substance ID: DTXSID20977346
• Nikkaji Number: J56.086C
• Mol file: 6177-60-2.mol

Synonyms:oxiran-2-ylmethyl methanesulfonate;6177-60-2;2,3-Epoxypropyl methanesulphonate;EINECS 228-223-0;(Oxiran-2-yl)methyl methanesulfonate;glycidyl mesylate;3-mesyloxy-1,2-epoxypropane;SCHEMBL1556223;Oxiranemethanol, methanesulfonate;DTXSID20977346;Methanesulfonic acid glycidyl ester;AKOS006271864;EN300-7164827

Chemical Property of 2,3-Epoxypropyl methanesulphonate

Chemical Property:

• Vapor Pressure: 0.00166mmHg at 25°C
• Refractive Index: 1.475
• Boiling Point: 303.6°C at 760 mmHg
• Flash Point: 137.4°C
• Density: 1.392g/cm³
• XLogP3: -0.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 152.01432991
• Heavy Atom Count: 9
• Complexity: 177

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CS(=O)(=O)OCC1CO1

Technology Process of 2,3-Epoxypropyl methanesulphonate

There total 2 articles about 2,3-Epoxypropyl methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxiranyl-methanol (556-52-5) + Methanesulfonic anhydride (7143-01-3) → S-(+)-3-mesyloxy-1,2-epoxypropane (6177-60-2)

Guidance literature:

With dmap; triethylamine; In ethyl acetate; at -5 - 20 ℃;

Reference yield:

→ S-(+)-3-mesyloxy-1,2-epoxypropane (6177-60-2)

Guidance literature:

Glycidol, CH3SO2Cl, (C2H5)3N/Toluol;

DOI:10.1246/bcsj.39.413

Reference yield: 85.0%

S-(+)-3-mesyloxy-1,2-epoxypropane (6177-60-2) → 2-Hydroxy-3-chlor-propyl-methan-sulfonat (6387-87-7)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

oxiranyl-methanol

Methanesulfonic anhydride

Downstream raw materials:

2-Hydroxy-3-chlor-propyl-methan-sulfonat

methanesulfonic acid

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