{[(3-chlorophenyl)amino]methylidene}propanedinitrile

Base Information

• Chemical Name: {[(3-chlorophenyl)amino]methylidene}propanedinitrile
• CAS No.: 6288-52-4
• Molecular Formula: C10H6 Cl N3
• Molecular Weight: 203.631

Synonyms:Malononitrile,[(m-chloroanilino)methylene]- (7CI,8CI); Propanedinitrile,[[(3-chlorophenyl)amino]methylene]- (9CI); NSC 11430; NSC 56178;[(m-Chloroanilino)methylene]malononitrile

Chemical Property of {[(3-chlorophenyl)amino]methylidene}propanedinitrile

Chemical Property:

• Vapor Pressure: 0.000187mmHg at 25°C
• Boiling Point: 328.7°C at 760 mmHg
• Flash Point: 152.6°C
• Density: 1.352g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of {[(3-chlorophenyl)amino]methylidene}propanedinitrile

There total 2 articles about {[(3-chlorophenyl)amino]methylidene}propanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-aniline (108-42-9) + Ethoxymethylenemalononitrile (123-06-8) → carbonyl cyanide m-chlorophenyl hydrazone (6288-52-4)

Guidance literature:

DOI:10.1021/ja01211a031

Reference yield:

→ carbonyl cyanide m-chlorophenyl hydrazone (6288-52-4)

Guidance literature:

entspr. Anilin, EtO-CH=C(CN)2;

Reference yield: 81.0%

4-toluenesulfonyl azide (941-55-9) + carbonyl cyanide m-chlorophenyl hydrazone (6288-52-4) + phenylacetylene (536-74-3) → N-[4-amino-1-(3-chlorophenyl)-5-cyano-3-phenylpyridin-2(1H)-ylidene]-4-methylbenzenesulfonamide

Guidance literature:

With copper(l) iodide; triethylamine; In tetrahydrofuran; at 25 ℃; for 1h; Sealed tube;

DOI:10.1021/ol4028368

upstream raw materials:

3-chloro-aniline

Ethoxymethylenemalononitrile

Downstream raw materials:

S-ethyl (2,2-dicyanovinyl)(m-chlorophenyl)thiocarbamate

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