(R)-Methyl 2,3-dihydroxypropanoate

Base Information

• Chemical Name: (R)-Methyl 2,3-dihydroxypropanoate
• CAS No.: 18289-89-9
• Molecular Formula: C4H8O4
• Molecular Weight: 120.105
• Mol file: 18289-89-9.mol

Synonyms:Methyl D-(-)-glycerate;(R)-Methyl 2,3-dihydroxypropanoate;

Chemical Property of (R)-Methyl 2,3-dihydroxypropanoate

Chemical Property:

• Boiling Point: 140 °C(Press: 15 Torr)
• PKA: 12.26±0.20(Predicted)
• PSA: 66.76000
• Density: 1.2795 g/cm3
• LogP: -1.48740
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

(R)-Methyl2,3-dihydroxypropanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (R)-Methyl 2,3-dihydroxypropanoate

There total 12 articles about (R)-Methyl 2,3-dihydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl (R)-2,2-dimethyl-1,3-dioxolane-4-carboxylate (52373-72-5) → methyl (2R)-2,3-dihydroxypropanoate (18289-89-9,15909-76-9)

Guidance literature:

With acetic acid; for 120h; Ambient temperature;

DOI:10.1021/jm00095a019

Reference yield: 94.0%

methanol (67-56-1) + D-glyceric acid (473-81-4,600-19-1,6000-40-4,28305-26-2,118916-26-0) → methyl (2R)-2,3-dihydroxypropanoate (18289-89-9,15909-76-9)

Guidance literature:

With hydrogenchloride;

DOI:10.1016/j.tetlet.2007.02.027

Reference yield: 44.0%

methyl glycidate (4538-50-5) → methyl (2R)-2,3-dihydroxypropanoate (18289-89-9,15909-76-9) + methyl (2S)-glycidate (4538-50-5,85485-00-3,111058-32-3,118712-39-3)

Guidance literature:

With water; In neat (no solvent); at 23 ℃; Reagent/catalyst; enantioselective reaction; Sealed tube;

DOI:10.1016/j.tet.2014.03.043

upstream raw materials:

methanol

glyceric acid

D-glyceric acid

methyl (R)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

Downstream raw materials:

methyl (2R)-2-methoxy-3-(triphenylmethoxy)propanoate

(R)-2-(4-vinyl-phenyl)-[1,3,2]dioxaborolane-4-carboxylic acid methyl ester

(R)-2-phenyl-[1,3,2]dioxaborolane-4-carboxylic acid methyl ester

methyl (R)-2,2-dimethyl-1,3-dioxolane-4-carboxylate

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