Mo₂Cl₄(chlorodiphenylphosphine)4

Base Information

• Chemical Name: Mo₂Cl₄(chlorodiphenylphosphine)4
• CAS No.: 115240-12-5
• Molecular Formula: C₄₈H₄₀Cl₈Mo₂P₄
• Molecular Weight: 1216.24
• Mol file: 115240-12-5.mol

Synonyms:

Chemical Property of Mo₂Cl₄(chlorodiphenylphosphine)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Mo₂Cl₄(chlorodiphenylphosphine)4

There total 4 articles about Mo₂Cl₄(chlorodiphenylphosphine)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + tetrakis(acetato)dimolybdenum(II) (14221-06-8,744215-74-5) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → Mo2Cl4(chlorodiphenylphosphine)4 (115240-12-5)

Guidance literature:

In dichloromethane; (N2); silane and P-compound added to suspn. of Mo-compound; stirred at room temp. for 30 min;; no solid isolated; Mo-complex detected by electronic spectrum;;

DOI:10.1016/S0020-1693(00)80974-3

Reference yield:

chloro-trimethyl-silane (75-77-4) + dimolybdenum(II) tetrakis(trifluoroacetate) (36608-07-8) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → Mo2Cl4(chlorodiphenylphosphine)4 (115240-12-5)

Guidance literature:

In dichloromethane; (N2); silane and P-compound added to suspn. of Mo-compound; stirred at room temp. for 30 min;; no solid isolated; Mo-complex detected by electronic spectrum;;

DOI:10.1016/S0020-1693(00)80974-3

Reference yield:

Cl8Mo2(4-) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → Mo2Cl4(chlorodiphenylphosphine)4 (115240-12-5)

Guidance literature:

(N2); no Mo2Cl4(PR3)4 formed in the reaction of Mo2Cl8(4-) with PClPh2;

DOI:10.1016/S0020-1693(00)80974-3

upstream raw materials:

chloro-trimethyl-silane

tetrakis(acetato)dimolybdenum(II)

chloro-diphenylphosphine

dimolybdenum(II) tetrakis(trifluoroacetate)