Benzenecarboximidic acid, N-methoxy-, phenylmethyl ester, (E)-

Base Information

Chemical Name:Benzenecarboximidic acid, N-methoxy-, phenylmethyl ester, (E)-
CAS No.:185197-24-4
Molecular Formula:C15H15NO2
Molecular Weight:241.29
Hs Code.:

Synonyms:

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Chemical Property of Benzenecarboximidic acid, N-methoxy-, phenylmethyl ester, (E)-

Chemical Property:

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Technology Process of Benzenecarboximidic acid, N-methoxy-, phenylmethyl ester, (E)-

There total 1 articles about Benzenecarboximidic acid, N-methoxy-, phenylmethyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: C₈H₈NO₂^(1-)*Ag⁽¹⁺⁾

: 22513-36-6
N-methoxy-N-(phenylmethyl)benzamide

: 185197-24-4
phenylmethyl (E)-N-methoxybenzimidate

: 185197-15-3
phenylmethyl (Z)-N-methoxybenzimidate

Guidance literature:: In diethyl ether; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2004.02.048

Reference yield: 31.0%

: 185197-24-4
phenylmethyl (E)-N-methoxybenzimidate

: 161869-74-5
(E)-2-hydroxy-1,2-diphenylethanone O-methyloxime

: 161869-75-6
(Z)-2-hydroxy-1,2-diphenylethanone O-methyloxime

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -23 ℃; for 0.5h;
DOI:10.1016/j.tet.2004.02.048

Reference yield:

: 185197-24-4
phenylmethyl (E)-N-methoxybenzimidate

: 530-36-9,3764-63-4,13286-63-0,23190-16-1,23190-17-2,23364-44-5,23412-95-5,39664-87-4,88082-66-0
erythro-2-amino-1,2-diphenylethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 31 percent / lithium diisopropylamide / tetrahydrofuran; hexane / 0.5 h / -23 °C

2: 100 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 20 °C

3: LiAlH₄ / tetrahydrofuran / 7 h / 0 °C

4: 40 mg / p-toluenesulfonic acid / methanol / 3 h / 20 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane; 1: imino 1,2-Wittig rearrangement;
DOI:10.1016/j.tet.2004.02.048