Diethyl piperidin-1-ylmethylphosphonate

Base Information

Chemical Name:Diethyl piperidin-1-ylmethylphosphonate
CAS No.:4972-40-1
Molecular Formula:C10H22NO3P
Molecular Weight:235.2603
Hs Code.:
NSC Number:202966
DSSTox Substance ID:DTXSID80308293
Wikidata:Q82056089

Synonyms:NSC202966;4972-40-1;DIETHYL PIPERIDIN-1-YLMETHYLPHOSPHONATE;SCHEMBL7450340;DTXSID80308293;NSC-202966;SR-01000195691;SR-01000195691-1

Suppliers and Price of Diethyl piperidin-1-ylmethylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Diethyl piperidin-1-ylmethylphosphonate

Chemical Property:

Vapor Pressure:0.000717mmHg at 25°C
Boiling Point:307.6°C at 760 mmHg
Flash Point:139.8°C
Density:1.062g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:235.13373056
Heavy Atom Count:15
Complexity:207

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOP(=O)(CN1CCCCC1)OCC

Technology Process of Diethyl piperidin-1-ylmethylphosphonate

There total 2 articles about Diethyl piperidin-1-ylmethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 626-67-5
N-methylcyclohexylamine

: 75-09-2
dichloromethane

: 762-04-9
phosphonic acid diethyl ester

: 4972-40-1
(piperidin-1-ylmethyl)phosphonic acid diethyl ester

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 12h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/jo501961h

Reference yield: 85.0%

: 110-89-4
piperidine

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 762-04-9
phosphonic acid diethyl ester

: 4972-40-1
(piperidin-1-ylmethyl)phosphonic acid diethyl ester

Guidance literature:

Reference yield:

: 4972-40-1
(piperidin-1-ylmethyl)phosphonic acid diethyl ester

: Diphenyl-(2-oxopiperidinomethyl)-phosphinoxid

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / diethyl ether

2: 23 percent / Hg(II)-EDTA / 1 h / 75 °C

With Hg(II)-EDTA; In diethyl ether;
DOI:10.1002/ardp.19893220709