(Methyl)tri-4-tolylphosphonium Iodide-d3,13C

Base Information

• Chemical Name: (Methyl)tri-4-tolylphosphonium Iodide-d3,13C
• CAS No.: 1896-61-3
• Molecular Formula: C22H24P.I
• Molecular Weight: 450.31500
• Mol file: 1896-61-3.mol

Synonyms:Methyl-tri-p-tolyl-phosphoniumiodid;Tri-n-propyl-methyl-zinn;methyl-tripropyl stannane;Tris-<4'-tolyl>-methyl-phosphonium;Methyl-tri-n-propylzinn;Methyl-tripropyl-stannan;methyl-tri-p-tolyl-phosphonium,iodide;methyl-tris(p-toluylphenyl)phosphonium iodide;Tris-(p-tolyl)-methyl-phosphoniumjodid;Stannane,methyltripropyl;Tri-p-tolyl-methylphosphoniumiodid;Methyl-tri-p-tolyl-phosphonium,Jodid;Methyl-tripropyl-zinn;Tripropylmethylstannan;

Chemical Property of (Methyl)tri-4-tolylphosphonium Iodide-d3,13C

Chemical Property:

• PSA: 13.59000
• LogP: 1.53950
• Solubility.: Ether

Purity/Quality:

98%,99%, ^*data from raw suppliers

(Methyl)tri-4-tolylphosphoniumIodide-d3,13C ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Methyl)tri-4-tolylphosphonium Iodide-d3,13C

There total 2 articles about (Methyl)tri-4-tolylphosphonium Iodide-d3,13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tri(p-tolyl)phosphine (1038-95-5,218281-19-7) + methyl iodide (74-88-4) → methyl-tris(p-toluylphenyl)phosphonium iodide (1896-61-3)

Guidance literature:

Reference yield:

→ methyl-tris(p-toluylphenyl)phosphonium iodide (1896-61-3)

Guidance literature:

aus Methyljodid u. Tri-p-tolyl-phosphin;

DOI:10.1016/0040-4020(68)89021-0

Reference yield: 46.0%

methyl-tris(p-toluylphenyl)phosphonium iodide (1896-61-3) + C55H95NO13Si2 → 24,33-Bis-(t.butyl-dimethylsilyl)-FK 506 (133941-75-0)

Guidance literature:

With epichlorohydrin; In 1,2-dichloro-benzene; at 140 ℃; for 0.05h;

DOI:10.1016/S0040-4039(02)02705-3

upstream raw materials:

Tri(p-tolyl)phosphine

methyl iodide

Downstream raw materials:

di(4-tolyl)methylphosphine oxide

toluene

24,33-Bis-(t.butyl-dimethylsilyl)-FK 506

C₅₆H₉₇NO₁₂Si₂

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