3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide

Base Information

Chemical Name:3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide
CAS No.:90316-38-4
Molecular Formula:C₁₃H₁₇NO₂
Molecular Weight:219.283
Hs Code.:
Wikidata:Q76324443

Synonyms:3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide;2-Butenamide, 3-(4-methoxyphenyl)-N,N-dimethyl-;90316-38-4;LS-46914

Suppliers and Price of 3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide

Chemical Property:

Vapor Pressure:3.39E-06mmHg at 25°C
Boiling Point:387.1°Cat760mmHg
Flash Point:187.9°C
Density:1.035g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:219.125928785
Heavy Atom Count:16
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC(=O)N(C)C)C1=CC=C(C=C1)OC
Isomeric SMILES:C/C(=C\C(=O)N(C)C)/C1=CC=C(C=C1)OC

Technology Process of 3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide

There total 7 articles about 3-(4-Methoxyphenyl)-N,N-dimethyl-2-butenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 29199-18-6
3-(4-methoxyphenyl)pentenedioic anhydride

: 124-40-3
dimethyl amine

: 90316-38-4
(E)-3-(4-methoxyphenyl)-N,N-dimethylbut-2-enamide

Guidance literature:: for 12h; Heating;

Reference yield:

: (E)-4-(dimethylamino)-4-oxobut-2-en-2-yl pivalate

: 93296-09-4
4-methoxyphenylzinc chloride

: 90316-38-4
(Z)-3-(4-methoxyphenyl)-N,N-dimethylbut-2-enamide

: 90316-38-4
(E)-3-(4-methoxyphenyl)-N,N-dimethylbut-2-enamide

Guidance literature:: With bis(tricyclohexylphosphine)nickel(II) dichloride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 25 ℃; for 24h; Overall yield = 99 %; Overall yield = 66 mg; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7ob02947k

Reference yield:

: (E)-4-(dimethylamino)-4-oxobut-2-en-2-yl pivalate

: 93296-09-4
4-methoxyphenylzinc chloride

: 90316-38-4
(Z)-3-(4-methoxyphenyl)-N,N-dimethylbut-2-enamide

: 90316-38-4
(E)-3-(4-methoxyphenyl)-N,N-dimethylbut-2-enamide

Guidance literature:: With bis(tricyclohexylphosphine)nickel(II) dichloride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 25 ℃; for 24h; Overall yield = 99 %; Overall yield = 66 mg; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7ob02947k