PHENANTHRENE,1,2,3,4-TETRA-

Base Information

• Chemical Name: PHENANTHRENE,1,2,3,4-TETRA-
• CAS No.: 1013-08-7
• Molecular Formula: C14H14
• Molecular Weight: 182.265
• Hs Code.: 2902909090
• Mol file: 1013-08-7.mol

Synonyms:PHENANTHRENE,1,2,3,4-TETRA-

Chemical Property of PHENANTHRENE,1,2,3,4-TETRA-

Chemical Property:

• Vapor Pressure: 0.000482mmHg at 25°C
• Melting Point: 33.5°C
• Refractive Index: 1.5372 (estimate)
• Boiling Point: 323.8°C at 760 mmHg
• Flash Point: 156.5°C
• PSA: 0.00000
• Density: 1.069g/cm³
• LogP: 3.71860

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PHENANTHRENE,1,2,3,4-TETRA-

There total 19 articles about PHENANTHRENE,1,2,3,4-TETRA- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

9,10-dihydrophenanthrene (776-35-2) → 1,2,3,4,4a,9,10,10a-octahydrophenanthrene (16306-39-1) + 1,2,3,4-tetrahydrophenanthrene (1013-08-7) + 1,2,3,4,5,6,7,8-Octahydrophenanthrene (5325-97-3)

Guidance literature:

With hydrogen; nickel; In water; ethylene glycol; at 80 ℃; Product distribution; 0.1M NaCl, 0.1M H₃BO₃, pH 2.6-2.7 to 6.0-6.4;

Reference yield: 11.0%

C14H13F → phenanthrene (85-01-8) + 1,2,3,4-tetrahydroanthracene (2141-42-6) + 1,2,3,4-tetrahydrophenanthrene (1013-08-7)

Guidance literature:

C₁₄H₁₃F; With boron trifluoride diethyl etherate; tetrakis(acetonitrile)palladium(II) bis(tetrafluoroborate); In various solvent(s); at 20 ℃; for 0.666667h;

With phosphate buffer; In various solvent(s); pH=7; Further stages.;

DOI:10.1021/ol702279w

Reference yield: 4.0%

phenanthrene (85-01-8) → 1,2,3,4,4a,9,10,10a-octahydrophenanthrene (16306-39-1) + 9,10-dihydrophenanthrene (776-35-2) + 1,2,3,4-tetrahydrophenanthrene (1013-08-7) + 1,2,3,4,5,6,7,8-Octahydrophenanthrene (5325-97-3)

Guidance literature:

With hydrogen; nickel; In water; ethylene glycol; at 80 ℃; Product distribution; 0.1M NaCl, 0.05M H₃BO₃, pH 2.7 to 10.4; also in different solvents with various supporting electrolytes, at various temperatures and current densities; influence of pH and buffer;

upstream raw materials:

phenanthrene

9,10-dihydroanthracene

9,10-dihydrophenanthrene

3,4-Dihydrophenanthrene

Downstream raw materials:

phenanthrene

3,4-dihydro-2H-phenanthren-1-one

2,3-Dihydro-4(1H)-phenanthrenone

2-Methylnaphthalene