Benzene, [(1E)-2-fluoroethenyl]-

Base Information

Chemical Name:Benzene, [(1E)-2-fluoroethenyl]-
CAS No.:20405-77-0
Molecular Formula:C8H7F
Molecular Weight:122.142
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, [(1E)-2-fluoroethenyl]-

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Technology Process of Benzene, [(1E)-2-fluoroethenyl]-

There total 34 articles about Benzene, [(1E)-2-fluoroethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 201230-82-2
carbon monoxide

: 118559-15-2
(E)-β-bromo-β-fluorostyrene

: 58041-00-2
(Z)-2-fluoro-3-phenylacrylaldehyde

: 20405-77-0
(E)-(2-fluorovinyl)benzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium formate; triphenylphosphine; In N,N-dimethyl-formamide; at 80 ℃; for 18h; under 30003 Torr; stereoselective reaction; Autoclave; Inert atmosphere;
DOI:10.1021/jo200798h

Reference yield: 76.0%

: 42599-24-6
E-styryl iodide

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 20405-77-0
(E)-(2-fluorovinyl)benzene

Guidance literature:: With N-fluoro-N-(tert-butyl)benzenesulfonamide; In tetrahydrofuran; diethyl ether; pentane; 1.) -120 deg C, 20 min; 2.) -120 deg C, 20 min then to r.t.;
DOI:10.1021/ja00269a052

Reference yield: 74.0%

: 6783-05-7
trans-2-phenylvinylboronic acid

: 20405-77-0
(E)-(2-fluorovinyl)benzene

Guidance literature:: trans-2-phenylvinylboronic acid; With sodium hydroxide; In methanol; at 23 ℃; for 0.25h; Inert atmosphere;

With silver trifluoromethanesulfonate; In methanol; at 0 ℃; for 0.5h; Inert atmosphere;

With Selectfluor; In acetone; at 23 ℃; for 1h; stereospecific reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol901113t