Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]-

Base Information

Chemical Name:Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]-
CAS No.:215033-50-4
Molecular Formula:C17H19NO
Molecular Weight:253.344
Hs Code.:
DSSTox Substance ID:DTXSID50425820
Nikkaji Number:J1.196.003K
Mol file:215033-50-4.mol

Synonyms:n-(3-tert-butylsalicylidene)aniline;215033-50-4;Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]-;SCHEMBL3775931;SCHEMBL3775934;SCHEMBL14750952;DTXSID50425820;2-tert-butyl-6-(phenyliminomethyl)phenol

Suppliers and Price of Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]-

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:253.146664230
Heavy Atom Count:19
Complexity:299

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC=CC(=C1O)C=NC2=CC=CC=C2

Technology Process of Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]-

There total 2 articles about Phenol, 2-(1,1-dimethylethyl)-6-[(phenylimino)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24623-65-2
3-tert-butyl-2-hydroxybenzaldehyde

: 62-53-3
aniline

: 215033-50-4
2-phenyliminomethyl-6-tert-butylphenol

Guidance literature:: With 3 A molecular sieve; In ethanol; at 20 ℃; for 16h;
DOI:10.1021/ja0032780

Reference yield:

: 88-18-6
2-tert-Butylphenol

: 215033-50-4
2-phenyliminomethyl-6-tert-butylphenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: EtMgBr / diethyl ether; tetrahydrofuran / 2 h / 20 °C

1.2: 82 percent / Et₃N / toluene / 2 h / 95 °C

2.1: 95 percent / 3 Angstroem sieves / ethanol / 16 h / 20 °C

With 3 A molecular sieve; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/ja0032780

Reference yield: 100.0%

: 75-77-4
chloro-trimethyl-silane

: 215033-50-4
2-phenyliminomethyl-6-tert-butylphenol

: 639806-66-9
N-[(3-tert-butyl-2-trimethylsilyloxy)phenyl]methylene aniline

Guidance literature:: 2-phenyliminomethyl-6-tert-butylphenol; With potassium hydride; In diethyl ether; at 20 ℃; for 2h; Schlenk technique; Inert atmosphere;

chloro-trimethyl-silane; In diethyl ether; at 20 ℃; for 20h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.poly.2016.07.033